Standard No.:	GB/T 23322-2009
Chinese Name:	纺织品 表面活性剂的测定 烷基酚聚氧乙烯醚
English Name:	Textiles - Determination of surfactant - Alkylphenol ethoxylates
Professional Classification:	GB National Standard
ICS Classification:	59.080.01 Textiles in general
Issued by:
Issued on:	2009-03-19
Implemented on:	2010-01-01
Status:	ABOLISHED
Replace By:	GB/T23322-2018 Textiles—Determination of surfactant—Alkylphenols and Alkylphenol ethoxylates
Replace By Date:	2019-07-01
Language:	English
File Format:	PDF
Word Count:	8000 words
Price(USD):	240 (USD)
Delivery:	via email in 1-3 business day

1 Scope

This standard specifies the screening method through reversed-phase high performance liquid chromatography (RHPLC), the determination method through normal phase high performance liquid chromatography (N-HPLC) and liquid chromatography - tandem mass spectrum (LC-MS/MS) all regarding alkylphenol polyoxyethylene (APnEO, n=2~16 ) in textiles.
This standard is applicable to various textile products.
Note: The general formula for molecular structure of APnEO is: R-C6H4-(OC2H4)nOH. The “APnEO” in this standard refers to common octaphenyl polyoxyethylene ether [OPnEO, C8H17-C6H4-(OC2H4)nOH] and nonylphenol polyoxyethylene ether [NPnEO, C9H19-C6H4-(OC2H4)nOH].

2 Principle

Extract APnEO in sample through Soxhlet extraction method with methyl alcohol serving as the extraction solvent, and after having concentrated and purified the extracting solution, determine such extracting solution with high-performance liquid chromatograph equipped with fluorescence detector or through liquid chromatography - tandem mass spectrum, then quantify with external standard method.

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